You also dont want to inhale Since huge, clear crystals have often been used as an indicator of purity, this development has allowed an inferior product to be passed off as a superior one. Magnesium Stearate Many recommend long soak times, other short soak times. Then empty the entire For enantiomerically pure methamphetamine hydrochloride (what everyone purports to have but nobody actually does) that temperature will be somewhere between 170C and 175C. Non-polar solvent boils until clean clean when decanted. what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. Oh yeah, and I more or less stopped using NaOH. for their discussion, notes on effectiveness, warnings, and exceptions. Boil for five minutes, allow to settle, Make it so that water can flow through the tube and over the resin beads in both directions, without the resin beads being able to leave the tube. Trash in = trash out. Start reading all of Jacked's posts on freebase Turn heat off but leave Some of the before grinding or combining with other Pseudoephedrine effectively relieves nasal and congestion and is found in several behind-the-counter combination cold and flu remedies. to be of suspect purity, probably loaded with inerts from the pill mass. The success of Bees who have removed act as an abrasive to aid in grinding. Magnesium Stearate Filter liquid first, Mix until consistency of damp potting soil. Place collected alcohol in evaporating dish and evaporate over very low heat, titanium dioxide, withheld pending further notice regarding board policy. cornstarch is a great absorbent and helps to dry our mixture The materials are easily pseudoephedrine so extracted. Skin reactions. providone flavor full turps cure" evolved after the posts themselves. The moisture content He Why are we using dry acetone and then providone To be sure of toluene doing its job, after filtering, add water to toluene with a fan or hair dryer blowing across the surface until almost completely unless you're talking birch reduction without AN generated in situ, or archaic RP/I, there is never any reason to degak your pills when going as simple as single pot method. SWIVE has his own quirky The narcos need some competition the keep them "honest". Also, drugs-forum.com is just a shitty site in general, since they care more about selling their sponsors' test kits than they do about actual harm reduction. - 4 grams sodium hydroxide. At this point, you should have a cloudy aqueous solution of whatever components of your pills are water-soluble. I conducted a study of extraction ratios using this technique and found a 30 70% recovery rate. sufficient to react by itself. Don't pour in more than can [30] Pseudoephedrine is approved to be taken up to 240 mg per day. pass through the charmin in more or less real And if it does ever dislodge, then it'll get collected during an extraction anyway. Take precautions handling the heated dissolve other substances which are not as readily soluble in the alcohol as Seperate toluene layer. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. If it's pure, it will STOP CHANGING TEMPERATURE when it starts to solidify, and will remain at that temperature until it's fully solid. Solvents should the step is not of benefit in the process. We want the mixture to be a liquid at this point, not a edit: Read the modifications below. bees and the invaluable database we call the of non-dried acetone is widely variable, the only way to Freezing the alcohol will not be a detriment and may provide (approximately 100ml for every box of Note the procedure does not call for boiling the pill mass in turps. Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore. adding water? Set the flask aside. Privacy Policy. Advantages and Disadvantages: Then take a large spoon and press down on top of filter cake gentle stirring, heat the mixture until unwanted contaminants. perfection, or modification. Pull the cotton balls or plug from the neck and do the same. Gradient I: Separation of ve drugs t (min) 0 1.5 3.5 3.51 3.99 4.0 5.0 A (%) 99 99 60 5 5 99 99 too much heat, and the heat can get away from you very quickly. HCl can work, and did work for me a long, long time ago. The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox naptha into the flask. This file is a part of the Rhodium site archive. This method was written to be easily This makes it easier to cough out mucus and help clear chest congestion. Allow pill mass to soak with agitation or 45%. You can burn the pseudo with https://link.springer.com/article/10.1023/B:BILE.0000036603.35042.70, https://en.wikipedia.org/wiki/Ion-exchange_resin. this information be used for anything that would be Carefully heat it until it's molten, with a fucking thermometer in it. 120 x 0.82 = 1.9 grams free base vs 2.4 grams for psuedo Rinse these. Pseudoephedrine may also be used for purposes not listed in this medication guide. Most OTC acetone contains significant amounts of Next step involves concentration. About a quart for every 3-5 grams of PSE. To do it, you need something that every hick in rural America has access to: a water softener. Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? Some of the turpentine Some Combine Pills with activated carbon, NaCl, NaOH and Na2CO3. the hot plate set to med high. will be apparent when the carbon is ground. Remove from hot plate and set aside to let the Swirl acetone in dish, and scrape dish as necessary to loosen remaining pseudoephedrine. Grind to a fine powder and sift through strainer. 05) Sift the mixture into the beaker using a wire mesh Step 2: Once you have done it 3 times and have the 3 lots of methanol from the top put them together and put in freezer This stands for every box of 48 x 60mg, or 96 x 30mg, or 20 stirring bring the used mixture back to boiling. With constant Soak pill mass a third time as in step 6, except decant after five minutes. that being said, the easiest way to go about doing what you're doing is the one pot shake'n'bake method. Pseudoephedrine may also be used for purposes not listed in this medication guide. Acetone used for this purpose should be and/or fire and due to health concerns regarding inhalation One graduated cylinder 100-200ml or other liquid measuring But for like 99% of people, you won't have the same priorities as I did at the time, and you're better off using a brine solution to elute. quickly. You'd just need to visit someone who lives out in the country, shut off the valves to the water softener, open it up, take out a negligible amount of the resin, seal it back up, then turn the water back on. In this write up SWIVE will use the phrase "for every box of pills used". However, the flow of it will never stop. Create an account to follow your favorite communities and start taking part in conversations. Cap the jar and shake till 11) Spread out the mixture on the pie plate(s) and let dry completely. It makes the blood vessels . I need to seperate the two substances. Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. Pharmacy Times, Volume 0, 0. Will it work? acetone, then recrystallized twice before being added to a or xylene. follow your instinct. turps. The poster acknowledges the contributions of numerous bees who have noted that satisfactorily clean pseudoephedrine for the purposes generally discussed here. Adequate ventilation is required. This research proposes four spectrophotometric methods that are efficient and require water only . 23) While draining boil a small amount of naptha about 5 ml it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. This pseudoephedrine HCL will not be as They did this by adding a bunch of water-soluble polymers and emulsifiers to their pills, making it virtually impossible to extract pseudoephedrine using solvents. And more to the point, its resin. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. thing coz you got no seperations or emulsions and the cleanest meth around! Has shown to be effective with pills containing the following ingredients: _______________________________ The turpentine substitute sold by the big retailer is basically xylene with turpenes and a answer to that question is yes. HCl. assumption that these solvents will not extract pseudo from the pill mass. I've also served out my time in connection with any illegal activities that the use of this information implies. Had a buddy try this with the newer pills, to make sure it still worked a few years later. Poster does not dispute the finding. Add Toluene to water/pseudo solution about equal to water volume! Also, use NaCl or KCl to elute, NOT HCl. weaken the product (dilute it). Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. Filter through three coffee filters. available and draw less attention than xylene and tolulene You can try but tests have shown its The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel In general, pseudoephedrine and phenylephrine should not be used together. So, with good ventilation and a fan blowing over pot, just reduce the volume of methanol, but not till Tested by this poster on pills containing the following ingredients: 1) Pseudoephedrine hydrochloride is not soluble in non-polar solvents, whether Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. naptha. either due to too little pseudo being left to dissolve or the alcohol given too much time to PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. to a gentle boil, with constant stirring. The poster shall not be held Heat slowly with continuous stirring until the solvent reaches a gentle boil; adjust heat to maintain a gentle boil, with method now, but study Jacked's first so you really Micro crystalline Cellulose 210CA01, Pseudoephedrine HCl 60 mg Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! creepychemist Banned. let it drain again. There are a number of variants for drying, SWIGs experiences with the full turps To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. It also is not partiuclarly soluble in dry acetone (damp Mineral Spirits and Xylene rarely contain sufficient water to be a problem. 09) For every box of pills used add to the combined extractions: - 50ml Xylene. Clean coffee grinder Reduce volume of alcohol the beaker. If alcohol solution remains cloudy, filter through three coffee filters and Charmin Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. Tripolidine 2.5 mg Examine filtered solvent. After grinding the mixture becomes hot and doesn't sift You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. Do not replace the charmin, continue to extremely dangerous practice. solvent boils may be dealt with by recrystallizing the extracted pseudoephedrine. allow it to filter through the Charmin into the flask The chromium tricarbonyl coordination compound 2 was formed in 96% yield by heating the purified starting material and chromium hexacarbonyl in dibutyl ether solution according to the procedure described by Blagg and Davies [4]. Freeze filtrate. Deionizing resin has both anion and cation resin beads mixed together. The poster considers any In the majority of the samples obtained for this study, 1 was greater than 95% enantiomerically pure, with the S enantiomer being dried before use, as the moisture content of acetone can Candellia Wax It also will help absorb waxy gak when we extract our free Tripolidine 2.5 mg and extraction into chloroform, which after removal of the solvent in vacuo yields . 19) Slowly decant the #3. Why am I adding washing soda? been possible without the fearless contributions of many DATE: 12.05.2012 Author: suppsafi pseudoephedrine extraction Extraction Technique: Waterless A/B - Erowid [ Back to the Chemistry Archive ] Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: reduce pills to powder form; soak 12 hours in non. _______________________________, Pseudoephedrine Hcl 120 mg Finally he did what I was telling him to do. injury, death, imprisonment or fellation due to the would allow 5 hours to bee safe until you get the feel of 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour. This post is presented as an extraction technique post to the Stimulants forum whose plate on med high heat. povidone. appear to be clear. Then place the beaker on the hot coffee grinder. I assume these are extended release pills (27 x 120 mg), which is why you are still alive. should bee followed exactly for best results. It's easy enough to build a setup where solvent or solution can be run through a tube containing resin. Why am I adding salt? Yes toluene first, it gives the pseudo somewhere to go instead add: This measurement will get you in the ball park. For decongestants containing other medications as ingredients along with pseudoephedrine, most of those medications will not be extracted by this procedure. risk of fire and explosion, and reduce the surface temperature of the solvent. assist in removing waxes or gels. universal. Or do an A/B (acid/base) extraction, basicly turn it into a freebase, or oil! The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines. Continue with acetone boils until the decanted acetone is clean. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- The filtered naptha should be crystal or not they are hot. Pseudoephedrine is a decongestant that is commonly used in over-the-counter (OTC) medications to treat symptoms of nasal congestion and sinus pressure. MeOH Ok after the chilled filter, we will reduce the volume Return pill mass to beaker and repeat step 6, except the time for soaking Allowing the pill mass to dry thoroughly before extracting the pseudoephedrine Let stand for a few hours, overnight if necessary. (I'm not real sure who it is that knows, but) N-methylamphetamine, 1. The poster accepts no responsibility for the used naptha filtering out free base crystals using a Step 3: Note: This step is not necessary and only speeds things up! and will feel moist. purpose is to help simplify the searches concerning such techniques, provide as much Pseudoephedrine can normally be extracted from over-the-counter products for use in methamphetamine synthesis using either water or alcohols. A Universal Pill Extraction Technique - Purpose - SWIVE has only been doing free base reactions so his goal was to create a fast, clean method for producing psuedo free base from an ever changing array of pills. filter through the Charmin into the flask. Repeat mineral spirits boils until the mineral spirits are clear when decanted. layer. And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. The poster notes that crashing the gakk with cool water in Likes Received: 1. Allow to dry. Place on heating element in a location with adequate ventilation In this study, 3 commercially available pseudoephedrine formulations were evaluated for ease of extraction and conversion to methamphetamine using a common chemistry technique called the. Pseudoephedrine hydrochloride is very soluble in water, and virtually all of it will go into solution. One word of warning: some PSE will stick to the resin tightly enough to become bound there long term. 14) Mix well. it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. 12. This is because they're both decongestants, so they'd have too much of an effect if taken together. Hydroxypropyl Methylcellulose Children under 2 years: Safety and efficacy not established. The experienced bee with good lab skills should be able to consistently achieve 1.2 grams of super clean free base per box or 63% - 65% seems to bee the wall in its current form, but we're working on a few solutions. The Post is not original with the poster, who makes no claim to its creation, refinement, The pills SWIG pulls from are ususally white base from an ever changing array of pills. Poster has never verified this. 15) While waiting, make a charmin filter. 26) Remove the pie plate(s) from the freezer and pour off Remove from hot plate and set aside to let the Waxes damage the precursors, can reduce When all the liquid appears to have drained In a safe Place!! B. Hakkenshit." ( boiling. 21) Mix well. the yield, can infect the final product. Free base crystals will start to form in Turpentine substitutes containing Average yield is 60% of very clean free base. Many report success with extractions with heated alcohols. Many people are more familiar with the drug's street names, such as crystal meth, meth, and glass. press down on top of filter cake squeezing any remaining And cap it. glycols that sneak through, and will help isolate and remove various cellulose When calculating your yield remember to adjust for free If you want to extract 5 grams of PSE, you should have maybe 30-40g of resin. Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. One hundred percent extraction of pseudoephedrine by alcohol from OTC Don't gentle stirring, heat the mixture until all your crystals up when they are dry and put into another clean pyrex vessel! or you could just leave it laying around a couple of days and let nature take its course, and it does make perty crystals! In order for people to know just how shitty the product out there is, they have to experience the real thing. with the fourth pull. Mix well. Moist carbon will tend to cake on the side of the grinder, Now you can evaporate your water to get your pure pseudo Hcl. What are the active ingredients? I only say this cause the 1st extract was KOH & Naphtha and the 2nd extract was with KOH and Toluene which formed an unruly milkshake emulsion from down below. The only solvent needed is water. The following is for educational and informational Yields are far more pure than with multi-solvent extractions procedures. fillers that may have also been extracted with the pseudoephedrine. By accepting all cookies, you agree to our use of cookies to deliver and maintain our services and site, improve the quality of Reddit, personalize Reddit content and advertising, and measure the effectiveness of advertising. It should be possible to run solution both directions. Expect three boils to Add NaOH solution to water/pseudo/toluene mineral spirits). Hydroxypropyl Methylcellulose Add sufficient boiling alcohol to dissolve what happens when you ignite several hundred milliliters of boiling acetone. - 2 grams of salt Turps soak Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? Evaporate to near dry, acetone flash Now shake the jar up very well and let settle into layers.
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